HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Chloro-1-methyl-4-nitroimidazole → HCID 86734275, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Chloro-1-methyl-4-nitroimidazole | HCID 21010 | — |
| Reactant | HCID 86734276 | HCID 86734276 | — |
| Reactant | HCID 178418582 | HCID 178418582 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 86734275 | HCID 86734275 | 91% |
Reaction Steps
The procedure was the same as that for 7c except that 800 mg (0.0024 mol) of 2, 160 mg of NaOCH3, and 400 mg of 5-chloro-1-methyl-4-nitroimidazole were used. The product obtained by crystallization from MeOH--H2O was dried over Drierite in vacuo at the temperature of refluxing toluene for 2 hr. to yield 1.0 g (91%) of 3c: mp 148° softens to a glass.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998806 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-8fa321d908b142d597a89f1ca1faf7e7 |
| Source note | uspto-grants-1976_12 |