HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl glycidyl ether → HCID 21430324, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl glycidyl ether | HCID 31217 | — |
| Reactant | N~1~,N~1~-Diphenylethane-1,2-diamine | HCID 13222166 | — |
| Product | HCID 21430324 | HCID 21430324 | — |
Reaction Steps
A mixture of 6.4 g. N-(2-aminoethyl)-diphenylamine and 4.7 g. 1,2-epoxy-3-phenoxy-propane was heated for 10 minutes at 160°C. The reaction product was triturated with ether and then recrystallized from isopropanol. 4.7 g. (43% of theory) of colorless crystals of 1-(2-diphenylaminoethylamino)-2-hydroxy-3-phenoxy-propane were obtained; m.p. 95° - 96°C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998810 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-e461e31c606a41ba8bb0a9b3768d9b57 |
| Source note | uspto-grants-1976_12 |