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HRID1973641

反应详情

EQUATION

反应方程式

HRID 1973641 的结构方程式

REACTANTS

反应物

2
结构：O=S(Cl)Cl
HCID24386

Thionyl chloride

Cl2OS

结构：O=C(O)CSCC(F)(F)F
HCID16790808

[(2,2,2-Trifluoroethyl)sulfanyl]acetic acid

C4H5F3O2S

PRODUCTS

生成物

1
结构：O=C(Cl)CSCC(F)(F)F
HCID21816785

[(2,2,2-Trifluoroethyl)sulfanyl]acetyl chloride

C4H4ClF3OS

PROCEDURE

实验过程

Thionyl chloride (21.9 g, 184 mmol) and trifluoroethylmercaptoacetic acid (15.9 g; 91 mmol) were stirred together overnight. The excess reagent was removed in vacuo and the product was distilled; bp 62°-68°/20 mm.

WORKUP

后处理

  1. customThe excess reagent was removed in vacuo
  2. distillationthe product was distilled