HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → [(2,2,2-Trifluoroethyl)sulfanyl]acetyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | 2-[(2,2,2-Trifluoroethyl)sulfanyl]acetic acid | HCID 16790808 | — |
| Product | [(2,2,2-Trifluoroethyl)sulfanyl]acetyl chloride | HCID 21816785 | — |
Reaction Steps
Thionyl chloride (21.9 g, 184 mmol) and trifluoroethylmercaptoacetic acid (15.9 g; 91 mmol) were stirred together overnight. The excess reagent was removed in vacuo and the product was distilled; bp 62°-68°/20 mm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998818 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-a7f62426647e4b4db636c8e32915a959 |
| Source note | uspto-grants-1976_12 |