HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethylamine → HCID 86734303, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethylamine | HCID 8021 | — |
| Reactant | HCID 86734304 | HCID 86734304 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 86734303 | HCID 86734303 | — |
Reaction Steps
3α-hydroxy-21-iodo-acetoxymethyl-5α-pregnane-11,20-dione (235 mg) in dry dichloromethane (25 ml) was treated with diethylamine (1 ml) in similar manner to that described in Example 35 to give title compound (89 mg)[αD ] + 73° (c 0.42).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998829 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-6f7704490fdf4e88832e74bfe3e218b2 |
| Source note | uspto-grants-1976_12 |