HuagongsheHuagongshe Chemistry Print Report · For research reference only
p-Toluenesulfonyl isocyanate → 5-sec.-BUTYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | p-Toluenesulfonyl isocyanate | HCID 77703 | — |
| Reactant | 5-(Butan-2-yl)cyclohexane-1,3-dione | HCID 20325617 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | 5-sec.-BUTYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE | HCID 20325621 | — |
Reaction Steps
Reaction of equimolar amounts of 5-sec.-butyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-sec.-BUTYL-2-(N-p-TOLUENESULFONYLCARBAMOYL)-1,3-CYCLOHEXANEDIONE, m.p. 92°-93° C. (corr.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998879 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-7baf7702d08d41cfa54342a1fc595719 |
| Source note | uspto-grants-1976_12 |