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HRID1973766

反应详情

EQUATION

反应方程式

HRID 1973766 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(S(=O)(=O)N=C=O)cc1
HCID77703

p-Toluenesulphonyl isocyanate

C8H7NO3S

结构：O=C1CC(=O)CC(c2ccccc2)C1
HCID568962

1,3-Cyclohexanedione, 5-phenyl-

C12H12O2

PRODUCTS

生成物

1
结构：Cc1ccc(S(=O)(=O)NC(=O)C2C(=O)CC(c3ccccc3)CC2=O)cc1
HCID20325601

N-[(4-Methylphenyl)sulfonyl]-2,6-dioxo-4-phenylcyclohexanecarboxamide

C20H19NO5S

AUXILIARIES

试剂、催化剂与溶剂

1
结构：c1ccccc1
溶剂HCID241

Benzene

C6H6

PROCEDURE

实验过程

Reaction of equimolar amounts of 5-phenyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-PHENYL-2-[N-p-TOLUENESULFONYLCARBAMOYL]-1,3-CYCLOHEXANEDIONE, m.p. 163.5°-166° C. (corr.).