HuagongsheHuagongshe Chemistry Print Report · For research reference only
Allylamine → HCID 21490733, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Allylamine | HCID 7853 | — |
| Reactant | HCID 131710580 | HCID 131710580 | — |
| Product | HCID 21490733 | HCID 21490733 | — |
Reaction Steps
A mixture of tetrahydrohomophthalic acid (9.2 g., 0.05 mole) and allylamine (2.8 g., 0.05 mole) is heated by an oil bath until molten for 40 minutes. The mixture solidifies upon cooling, and is recrystallized twice from isopropanol, giving 2-allyl-5,6,7,8-tetrahydroisoquinoline-1,3(2H, 4H)-dione.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US03998954 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-dc18d779806e4351ac8fc00a11e9100e |
| Source note | uspto-grants-1976_12 |