Triethyl orthoacetate → HCID 21488582, compound

HRID 1974064Notes

Reaction equation

HRID 1974064 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]2[C:11](=[CH:12][CH:13]=1)[N:10]=[C:9]([NH:14][NH2:15])[CH:8]=[C:7]2[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[Cl:22])([O-:3])=[O:2].[C:23](OCC)(OCC)(OCC)[CH3:24]>C1(C)C(C)=CC=CC=1>[N+:1]([C:4]1[CH:5]=[C:6]2[C:11](=[CH:12][CH:13]=1)[N:10]1[C:23]([CH3:24])=[N:15][N:14]=[C:9]1[CH:8]=[C:7]2[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][C:17]=1[Cl:22])([O-:3])=[O:2]

Participants

4

Reactant 2

HCID 66221Triethyl orthoacetateHCID 21488581HCID 21488581, compound

Product 1

HCID 21488582HCID 21488582, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

In the manner given in Example 2, 6-nitro-4-(o-chlorophenyl)-2-hydrazinoquinoline, and triethyl orthoacetate are refluxed in xylene to give 7-nitro-1-methyl-5-(o-chlorophenyl)-s-triazolo[4,3-a]quinoline.

Sources & evidence

ORD record
ord-4962df3ee2f542f79e4611e1b3a092d1
Source dataset
uspto-grants-1976_12
Patent number
US04000151

Reaction notes

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