Triethyl orthoacetate → HCID 21488585, compound

HRID 1974070Notes

Reaction equation

HRID 1974070 reaction equation
[F:1][C:2]([F:23])([F:22])[C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[N:9]=[C:8]([NH:13][NH2:14])[CH:7]=[C:6]2[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[Cl:21].[C:24](OCC)(OCC)(OCC)[CH3:25]>C1(C)C(C)=CC=CC=1>[F:23][C:2]([F:1])([F:22])[C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[N:9]1[C:24]([CH3:25])=[N:14][N:13]=[C:8]1[CH:7]=[C:6]2[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][C:16]=1[Cl:21]

Participants

4

Reactant 2

HCID 66221Triethyl orthoacetateHCID 21488600HCID 21488600, compound

Product 1

HCID 21488585HCID 21488585, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

In the manner given in Example 2, 6-(trifluoromethyl)-4-(o-chlorophenyl)-2-hydrazinoquinoline and triethyl orthoacetate are refluxed in xylene to give 7-(trifluoromethyl)-1-methyl-5-(o-chlorophenyl)-s-triazolo[4,3-a]quinoline

Sources & evidence

ORD record
ord-c2661cf1766042c9a8dc45fca6d7bd86
Source dataset
uspto-grants-1976_12
Patent number
US04000151

Reaction notes

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