Hydrazine hydrate (1:1) → HCID 21488597, compound

HRID 1974072Notes

Reaction equation

HRID 1974072 reaction equation
Cl[C:2]1[CH:11]=[C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([N+:18]([O-:20])=[O:19])[CH:8]=2)[N:3]=1.O.[NH2:22][NH2:23]>>[N+:18]([C:7]1[CH:8]=[C:9]2[C:4](=[CH:5][CH:6]=1)[N:3]=[C:2]([NH:22][NH2:23])[CH:11]=[C:10]2[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1)([O-:20])=[O:19]

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 21488599HCID 21488599, compound

Product 1

HCID 21488597HCID 21488597, compound

Procedure

In the manner given in Example 1, 2-chloro-6-nitro-4-phenylquinoline is reacted at reflux with hydrazine hydrate to give 6-nitro-4-phenyl-2-hydrazinoquinoline.

Workup

  1. customis reacted

Sources & evidence

ORD record
ord-b378bf65e801406aa542d5783d561e94
Source dataset
uspto-grants-1976_12
Patent number
US04000151

Reaction notes

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