Triethyl orthoacetate → HCID 21488576, compound

HRID 1974073Notes

Reaction equation

HRID 1974073 reaction equation
[N+:1]([C:4]1[CH:5]=[C:6]2[C:11](=[CH:12][CH:13]=1)[N:10]=[C:9]([NH:14][NH2:15])[CH:8]=[C:7]2[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)([O-:3])=[O:2].[C:22](OCC)(OCC)(OCC)[CH3:23]>C1(C)C(C)=CC=CC=1>[N+:1]([C:4]1[CH:5]=[C:6]2[C:11](=[CH:12][CH:13]=1)[N:10]1[C:22]([CH3:23])=[N:15][N:14]=[C:9]1[CH:8]=[C:7]2[C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1)([O-:3])=[O:2]

Participants

4

Reactant 2

HCID 66221Triethyl orthoacetateHCID 21488597HCID 21488597, compound

Product 1

HCID 21488576HCID 21488576, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

In the manner given in Example 2, 6-nitro-4-phenyl-2-hydrazinoquinoline and triethyl orthoacetate are refluxed in xylene to give 7-nitro-1-methyl-5-phenyl-s-triazolo[4,3-a]quinoline.

Sources & evidence

ORD record
ord-00900279adbd4fe79758e19e2ddeb000
Source dataset
uspto-grants-1976_12
Patent number
US04000151

Reaction notes

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