Triethyl orthoacetate → HCID 21488614, compound

HRID 1974076Notes

Reaction equation

HRID 1974076 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8]1[C:17]2[C:12](=[CH:13][CH:14]=[CH:15][CH:16]=2)[N:11]=[C:10]([NH:18][NH2:19])[CH:9]=1.[C:20](OCC)(OCC)(OCC)[CH3:21]>C1(C)C(C)=CC=CC=1>[CH3:20][C:21]1[N:11]2[C:12]3[C:17]([C:8]([C:3]4[CH:4]=[CH:5][CH:6]=[CH:7][C:2]=4[Cl:1])=[CH:9][C:10]2=[N:18][N:19]=1)=[CH:16][CH:15]=[CH:14][CH:13]=3

Participants

4

Reactant 2

HCID 66221Triethyl orthoacetateHCID 21488617HCID 21488617, compound

Product 1

HCID 21488614HCID 21488614, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

In the manner given in Example 2, 4-(o-chlorophenyl)-2-hydrazinoquinoline and triethyl orthoacetate are refluxed in xylene to give 1-methyl-5-(o-chlorophenyl)-s-triazolo[4,3-a]quinoline.

Sources & evidence

ORD record
ord-1edd08a6a64b4a8c8221d104e9582fde
Source dataset
uspto-grants-1976_12
Patent number
US04000151

Reaction notes

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