Hydrazine hydrate (1:1) → 6-Chloro-2-hydrazinyl-4-phenylquinoline

HRID 1974078Notes

Reaction equation

HRID 1974078 reaction equation
Cl[C:2]1[CH:11]=[C:10]([C:12]2[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=2)[C:9]2[C:4](=[CH:5][CH:6]=[C:7]([Cl:18])[CH:8]=2)[N:3]=1.O.[NH2:20][NH2:21]>>[Cl:18][C:7]1[CH:8]=[C:9]2[C:4](=[CH:5][CH:6]=1)[N:3]=[C:2]([NH:20][NH2:21])[CH:11]=[C:10]2[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1

Participants

3

Reactant 2

HCID 24654Hydrazine hydrate (1:1)HCID 43246192,6-dichloro-4-phenylquinoline

Product 1

HCID 126119386-Chloro-2-hydrazinyl-4-phenylquinoline

Procedure

In the manner given in Example 1, 2,6-dichloro-4-phenylquinoline is reacted at reflux with hydrazine hydrate to give 6-chloro-4-phenyl-2-hydrazinoquinoline.

Workup

  1. customis reacted

Sources & evidence

ORD record
ord-2840b4b466d24522bb338bff62b3278a
Source dataset
uspto-grants-1976_12
Patent number
US04000151

Reaction notes

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