HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl orthoformate → [1,2,4]Triazolo[4,3-a]quinoline, 7-chloro-5-phenyl-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | 6-Chloro-2-hydrazinyl-4-phenylquinoline | HCID 12611938 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | [1,2,4]Triazolo[4,3-a]quinoline, 7-chloro-5-phenyl- | HCID 12246499 | — |
Reaction Steps
In the manner given in Example 2, 6-chloro-4-phenyl-2-hydrazinoquinoline and triethyl orthoformate are refluxed in xylene to give 7-chloro-5-phenyl-s-triazolo[4,3-a]quinoline of melting point 265°-266.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04000151 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-7a82c094e19a4816bc8405ccd17b37a6 |
| Source note | uspto-grants-1976_12 |