Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methyl iodide | HCID 6328 | — |
| Reactant | HCID 20559958 | HCID 20559958 | — |
| Reactant | 18820-83-2 | HCID 21863515 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20560070 | HCID 20560070 | — |
Reaction Steps
A solution of 2-(o-formamidophenethyl)pyridine (55 g., 0.243 mole) and methyl iodide (38 g., 0.268 mole) in 500 ml. of acetone is refluxed for 20 hours. The mixture is cooled at 5° C. and filtered to provide 82 g. (92%) of the pyridinium iodide having melting point of 199.5°-201.5° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04000143 |
|---|
| Source dataset | uspto-grants-1976_12 |
|---|
| ORD ID | ord-cc4efc4fb9ff41a18c02a1145f7e179d |
|---|
| Source note | uspto-grants-1976_12 |
|---|
