Formaldehyde → HCID 21488670, compound

HRID 1974156Notes

Reaction equation

HRID 1974156 reaction equation
[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:21])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[N:15]1[CH:19]=[N:18][N:17]=[C:16]1[CH3:20].[CH2:22]=[O:23]>C1(C)C(C)=CC=CC=1>[Cl:1][C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][C:3]=1[C:8](=[O:21])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][C:10]=1[N:15]1[C:16]([CH3:20])=[N:17][N:18]=[C:19]1[CH2:22][OH:23]

Participants

4

Reactant 2

HCID 712FormaldehydeHCID 21488589HCID 21488589, compound

Product 1

HCID 21488670HCID 21488670, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Conditions

Temperature
122 °C

Procedure

In the manner given in Example 4, 2'-chloro-2-(3-methyl-4H-1,2,4-triazol-4-yl)benzophenone, paraformaldehyde and xylene are warmed under nitrogen to about 122° C. to give 2'-chloro-2-[3-(hydroxymethyl)-5-methyl-4H-1,2,4-triazol-4-yl]benzophenone.

Sources & evidence

ORD record
ord-1bc2d14e18354752ad9a10635b9f6390
Source dataset
uspto-grants-1976_12
Patent number
US04000153

Reaction notes

Loading…