Triethyl orthoacetate → HCID 21488644, compound

HRID 1974164Notes

Reaction equation

HRID 1974164 reaction equation
[Br:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[N:8]=[C:7]([NH:12][NH2:13])[CH:6]=[C:5]2[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1.[C:20](OCC)(OCC)(OCC)[CH3:21]>C1(C)C(C)=CC=CC=1>[Br:1][C:2]1[CH:3]=[C:4]2[C:9](=[CH:10][CH:11]=1)[N:8]1[C:20]([CH3:21])=[N:13][N:12]=[C:7]1[CH:6]=[C:5]2[C:14]1[CH:19]=[CH:18][CH:17]=[CH:16][CH:15]=1

Participants

4

Reactant 2

HCID 66221Triethyl orthoacetateHCID 14914943HCID 14914943, compound

Product 1

HCID 21488644HCID 21488644, compound

Reagents, catalysts & solvents 1

HCID 7237O-XyleneSolvent

Procedure

In the manner given in Example 2, 6-bromo-4-phenyl-2-hydrazinoquinoline and triethyl orthoacetate are refluxed in xylene to give 7-bromo-1-methyl-5-phenyl-s-triazolo[4,3-a]quinoline.

Sources & evidence

ORD record
ord-46f921819a7c4267921bb11f287e564d
Source dataset
uspto-grants-1976_12
Patent number
US04000153

Reaction notes

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