Vinyl Chloride → HCID 86734336, compound
Reaction equation
[CH:1]([Cl:3])=[CH2:2].[C:4]([O:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])(=[O:8])[C:5]([CH3:7])=[CH2:6].C(OOC(=O)C1C=CC=CC=1)(=O)C1C=CC=CC=1>CC(C)=O>[C:4]([O:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH3:21])(=[O:8])[C:5]([CH3:7])=[CH2:6].[CH:1]([Cl:3])=[CH2:2]Participants
5
Reactant 3
Product 1
Reagents, catalysts & solvents 1
Conditions
- Temperature
- 51 °C
Procedure
150 parts of acetone, 71.1 parts of vinyl chloride, 28.9 parts of lauryl methacrylate and 1.5 parts of benzoyl peroxide were charged to an autoclave and heated to 51° C. for 154 hours. The resulting slurry was washed thoroughly with isopropanol, centrifuged and dried for 64 hours at 30° C. and 2.0 mm. Hg. There was obtained a lauryl methacrylate/vinyl chloride copolymer interfacial agent (about 90% conversion) product. Said interfacial agent was a dry white powder and had a reduced viscosity of 0.29 dl./g. as measured on a solution of 0.2 grams in 100 ml. of benzene at 30° C.
Workup
- washThe resulting slurry was washed thoroughly with isopropanol
- customdried for 64 hours at 30° C.
Sources & evidence
- ORD record
- ord-2a8e7da29ce14d058f3aab61326291c5
- Source dataset
- uspto-grants-1976_12
- Patent number
- US04000218
Reaction notes
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