Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Vinyl Chloride | HCID 6338 | — |
| Reactant | Benzoyl Peroxide | HCID 7187 | — |
| Reactant | Lauryl Methacrylate | HCID 8906 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 86734336 | HCID 86734336 | — |
Reaction Steps
150 parts of acetone, 71.1 parts of vinyl chloride, 28.9 parts of lauryl methacrylate and 1.5 parts of benzoyl peroxide were charged to an autoclave and heated to 51° C. for 154 hours. The resulting slurry was washed thoroughly with isopropanol, centrifuged and dried for 64 hours at 30° C. and 2.0 mm. Hg. There was obtained a lauryl methacrylate/vinyl chloride copolymer interfacial agent (about 90% conversion) product. Said interfacial agent was a dry white powder and had a reduced viscosity of 0.29 dl./g. as measured on a solution of 0.2 grams in 100 ml. of benzene at 30° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US04000218 |
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| Source dataset | uspto-grants-1976_12 |
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| ORD ID | ord-2a8e7da29ce14d058f3aab61326291c5 |
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| Source note | uspto-grants-1976_12 |
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