HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-((Bis(benzyl)amino)acetyl)salicylamide → HCID 21488956, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-((Bis(benzyl)amino)acetyl)salicylamide | HCID 121727 | — |
| Reactant | 2H-Pyran, 2-(4-chlorobutoxy)tetrahydro- | HCID 170488 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | HCID 21488956 | HCID 21488956 | — |
Reaction Steps
A mixture of 5-(N,N-dibenzylglycyl)salicylamide, sodium salt (3.96 g), 2-(4-chlorobutoxy)tetrahydropyran (1.92 g) sodium iodide (1.40 g) and butanone (100 ml) was heated under reflux for 30 hours and filtered. The filtrate was evaporated to give an oil which crystallised from isopropanol to afford the ether as colourless crystals (2.95 g), m.p. 118°-123°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04000193 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-d8644fe7c0a14aa78563ec3b8957f6ad |
| Source note | uspto-grants-1976_12 |