HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Nitro-N-(pyridin-4-yl)pyridin-2-amine → HCID 12445535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Nitro-N-(pyridin-4-yl)pyridin-2-amine | HCID 12445392 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 12445535 | HCID 12445535 | — |
Reaction Steps
The nitro compound from Step A (1.0 g.) was hydrogenated in 60 ml. of methanol over 0.2 g. of 5% palladium on carbon catalyst. The catalyst was removed by filtration and the filtrate was evaporated to dryness.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04000286 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-ea124cf1a6c54326bf7e664de0c6bc0c |
| Source note | uspto-grants-1976_12 |