Dl-Tryptophan → HCID 53644392, compound

HRID 1974340Notes

Reaction equation

HRID 1974340 reaction equation
[C:1]1([CH3:8])[CH:6]=[CH:5][C:4](Cl)=[CH:3][CH:2]=1.[NH2:9][CH:10]([C:21]([OH:23])=[O:22])[CH2:11][C:12]1[C:20]2[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=2)[NH:14][CH:13]=1>>[C:1]1([CH3:8])[CH:6]=[CH:5][C:4]([NH:9][CH:10]([C:21]([OH:23])=[O:22])[CH2:11][C:12]2[C:20]3[C:15](=[CH:16][CH:17]=[CH:18][CH:19]=3)[NH:14][CH:13]=2)=[CH:3][CH:2]=1

Participants

3

Reactant 2

HCID 1148Dl-TryptophanHCID 78104-Chlorotoluene

Product 1

HCID 53644392HCID 53644392, compoundYield 82%

Procedure

The same procedure is used as in Example 1, p-toluyl chloride and DL-tryptophane being used. Yield 82%. Melting point 217.5° to 218.5° C.

Sources & evidence

ORD record
ord-00f84de7f1734280aa7157daf8b21064
Source dataset
uspto-grants-1976_12
Patent number
US04000297

Reaction notes

Loading…