HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl isothiocyanate → HCID 178465516, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl isothiocyanate | HCID 10966 | — |
| Reactant | HCID 178433288 | HCID 178433288 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 178465516 | HCID 178465516 | 86.4% |
Reaction Steps
(i) A solution of 4-methyl-5-[(2-aminoethyl)thiomethyl]-imidazole (6.9 g) and ethyl isothiocyanate (3.84 g) in ethanol was heated under reflux for 2 hours. Concentration followed by recrystallisation of the residue from aqueous ethanol gave N-ethyl-N'-[2-((4-methyl-5-imidazolyl)methylthio)ethyl]thiourea (9.0 g), m.p. 140°-141°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04000302 |
| Source dataset | uspto-grants-1976_12 |
| ORD ID | ord-88b59d6d40154dca9f82e126b804ec94 |
| Source note | uspto-grants-1976_12 |