HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Nitrate → HCID 19101553, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Nitrate | HCID 24434 | — |
| Reactant | HCID 19101592 | HCID 19101592 | — |
| Solvent | Sulfuric Acid | HCID 1118 | — |
| Product | HCID 19101553 | HCID 19101553 | 78.5% |
Reaction Steps
To a solution of 1 g of 7-(1-imidazolyl)-1-n-propylquinoxaline-2,3-(1H,4H)-dione hydrochloride in 8 ml of sulfuric acid was added 0.4 g of potassium nitrate, and the mixture was stirred overnight. The reaction mixture was poured in ice-water and adjusted to pH 7. The resulting crystals were recrystallized from 1N-hydrochloric acid to provide 0.9 g of 7-(1-imidazolyl)-6-nitro-1-n-propylquinoxaline-2,3-(1H,4H)-dione hydrochloride.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05283244 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-20ebe5e129c04fe8b1faf16d50b327d4 |
| Source note | uspto-grants-1994_02 |