3-Amino-1-propanol → HCID 18990341, compound

HRID 1974745Notes

Reaction equation

HRID 1974745 reaction equation
C([O:4][C:5]1[CH:6]=[C:7]([CH:11]=[C:12]([N+:18]([O-:20])=[O:19])[C:13]=1[O:14]C(=O)C)[C:8]([OH:10])=O)(=O)C.[NH2:21][CH2:22][CH2:23][CH2:24][OH:25]>>[OH:25][CH2:24][CH2:23][CH2:22][NH:21][C:8](=[O:10])[C:7]1[CH:11]=[C:12]([N+:18]([O-:20])=[O:19])[C:13]([OH:14])=[C:5]([OH:4])[CH:6]=1

Participants

3

Reactant 2

HCID 90863-Amino-1-propanolHCID 154807403,4-Diacetoxy-5-nitrobenzoic acid

Product 1

HCID 18990341HCID 18990341, compoundYield 85%

Procedure

The procedures described in Examples 43 and 44 were repeated using 3,4-diacetoxy-5-nitrobenzoic acid and 3-aminopropan-1-ol. Yield 85%, m.p. 160°-163° C.

Sources & evidence

ORD record
ord-8e4674fb6e80442abb8b46783ceb284a
Source dataset
uspto-grants-1994_02
Patent number
US05283352

Reaction notes

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