反应详情

The compound 2-[2-(4-fluorophenylthio)-6-fluorophenyl]-4,4-dimethyloxazoline (5.0 g, 15.66 mmol) is added to 310 ml of a 4.5N HCl solution in water and is refluxed overnight. The cooled reaction mixture is extracted twice with ethyl acetate. The extracts are washed with water and then brine and dried over MgSO4 to afford the subtitle compound.

1. temperatureis refluxed overnight
2. customThe cooled reaction mixture
3. extractionis extracted twice with ethyl acetate
4. washThe extracts are washed with water
5. dry with materialbrine and dried over MgSO4