HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 11199196, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Dichloromethane | HCID 6344 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 11199196 | HCID 11199196 | — |
Reaction Steps
After heating, the thick paste was diluted with 450 mL toluene, cooled in an ice/water bath and isolated by filtration. It was treated with portions of toluene and methylene chloride until the amount of residual phenol was less than 1 area percent by HPLC analysis. The solid was isolated by filtration and was 90% pure by HPLC analysis, product weight, 57.7 g (76%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05283374 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-1a8181b4940e41139a0522d0d467934e |
| Source note | uspto-grants-1994_02 |