Water → HCID 23233629, compound

Participants

Reaction Steps

26.5 g of 4-chloro-3-amino-N,N-bistrifluoromethyl-aminobenzene were dissolved in 50 g of toluene and reacted at 350° C. The reaction products were introduced into 150 ml of water. The two-phase mixture obtained was made alkaline with 20% strength by weight aqueous sodium hydroxide solution, and the toluene phase was separated off, to give 10.3 g of 3-amino-N,N-bistrifluoromethyl-aminobenzene of boiling point 76° to 78° C. at 20 mbar by distillation.

Provenance & Evidence