HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 57259964, compound → HCID 67641539, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 57259964 | HCID 57259964 | — |
| Reactant | HCID 86751143 | HCID 86751143 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 67641539 | HCID 67641539 | 85.6% |
Reaction Steps
(2S)-2-Amino-3,3-dimethyl-N,N-dimethylbutyramide hydrochloride (0.25 g), (2S)-2-chlorocarbonyloxy-4-methylvaleric acid benzyl ester (0.36 g) and TEA (0.31 g) were reacted in ethyl acetate (10 ml) in a similar manner to that of Example 4-1) to give (2S)-2-[N-[(1S)-2,2-dimethyl-1-(N,N-dimethylcarbamoyl)propyl]carbamoyloxy]-4-methylvaleric acid benzyl ester (0.44 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284828 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-58082ef33160458e803bb63d6a0ffb0b |
| Source note | uspto-grants-1994_02 |