HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19100956, compound → HCID 19100947, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19100956 | HCID 19100956 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19100947 | HCID 19100947 | — |
Reaction Steps
32 g (0.11 mol) of ethyl 2-benzyl-3-methyl-2,7-diazabicyclo[3.3.0]octane-7-carboxylate in 560 ml of ethanol are hydrogenated on 4.5 g of palladium/active carbon at 100° C. and 100 bar. The catalyst is filtered off with suction, the filtrate is concentrated, and the residue is distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284855 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-32243b3da3694e8fb1e0cc80261e3ae3 |
| Source note | uspto-grants-1994_02 |