HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19100950, compound → HCID 19100969, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19100950 | HCID 19100950 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 19100969 | HCID 19100969 | — |
Reaction Steps
13 g (44.9 mmol) of ethyl 2-benzyl-6-methyl-2,7-diazabicyclo[3.3.0]octane-7-carboxylate in 150 ml of ethanol are hydrogenated on 2 g of palladium/active carbon (10% Pd) at 100° C. and 100 bar. The catalyst is filtered off, and the filtrate is concentrated and distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284855 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-d51022f4a91d4b2caf70e7795369fac7 |
| Source note | uspto-grants-1994_02 |