HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19100964, compound → HCID 16228902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19100964 | HCID 19100964 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 16228902 | HCID 16228902 | — |
Reaction Steps
96.5 g (0.279 mol) of diethyl 2-benzyl-2,7-diazabicyclo[3.3.0]octane-3,7-dicarboxylate in 1 l of ethanol are hydrogenated on 5 g of palladium/active carbon (10% Pd) at 100° C. and 100 bar. The liquid phase is filtered off with suction, concentrated and distilled.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05284855 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-64f0a601855e417ca82902de6d16480f |
| Source note | uspto-grants-1994_02 |