HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sulfuric Acid → HCID 10656042, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sulfuric Acid | HCID 1118 | — |
| Reactant | HCID 10516025 | HCID 10516025 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 10656042 | HCID 10656042 | — |
Reaction Steps
To a stirred solution of glacial acetic acid (100 ml) and an aqueous solution of sulfuric acid (12.5%, 30 ml), there was added methyl 1-(2,4-difluorobenzyl)-2-oxocyclopentanecarboxylate (5.14 g, 21.6 mmol). The mixture was refluxed in a stream of argon for 5 h.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05286737 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-3e47b7460aa94e8985812e0ba23aa96c |
| Source note | uspto-grants-1994_02 |