HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2-Methylbenzyl)piperazine → HCID 19099445, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2-Methylbenzyl)piperazine | HCID 79212 | — |
| Reactant | 4-[N-(2-isopropyloxyethyl)-N-chloroacetylamino]benzoyl chloride | HCID 19099416 | — |
| Product | HCID 19099445 | HCID 19099445 | — |
Reaction Steps
Analogously to Example 55, 1.5 g of 4-[N-(2-isopropyloxyethyl)-N-chloroacetylamino]benzoyl chloride are reacted with 0.76 g of 2-methylbenzylpiperazine, yielding 1-{4-[N-(2-isopropyloxyethyl)-N-chloroacetylamino]benzoyl}-4-(2-methylbenzyl)piperazine. The hydrochloride thereof melts at 142°-143°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05286728 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-447d6f5c565c41e38004ca27f4f2976f |
| Source note | uspto-grants-1994_02 |