HuagongsheHuagongshe Chemistry Print Report · For research reference only
M-Cresol → 2-Propanamine, 1-(3-methylphenoxy)-
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | M-Cresol | HCID 342 | — |
| Reactant | 2-Methylaziridine | HCID 6377 | — |
| Solvent | Decane | HCID 15600 | — |
| Product | 2-Propanamine, 1-(3-methylphenoxy)- | HCID 12298896 | 57.5% |
Reaction Steps
21.6 Grams (0.20 mol) of m-cresol and 2.3 g (0.04 mol) of propyleneimine in 20 ml of n-decane were allowed to react in an autoclave at 5 kg/cm2G at 150° C. for 6 hours. Thereafter, the resultant reaction product was treated in the same manner as in Example 17 to give 3.8 g of 1-(3-methylphenoxy)-2-propylamine. Its yield was as high as 57%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05286905 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-e5b23485237f42d0aab5b0b75f82fc8f |
| Source note | uspto-grants-1994_02 |