p-Toluenesulfonic acid → HCID 23372105, compound
Reaction equation
[CH:1]1([O:7][N:8]2[C:13]([CH3:15])([CH3:14])[CH2:12][C:11](=[O:16])[CH2:10][C:9]2([CH3:18])[CH3:17])[CH2:6][CH2:5][CH2:4][CH2:3][CH2:2]1.[OH:19][CH2:20][C:21]([CH2:25]O)([CH2:23][OH:24])[CH3:22].C1(C)C=CC(S(O)(=O)=O)=CC=1>>[OH:19][CH2:20][C:21]1([CH3:25])[CH2:23][O:24][C:11]2([CH2:12][C:13]([CH3:14])([CH3:15])[N:8]([O:7][CH:1]3[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6]3)[C:9]([CH3:18])([CH3:17])[CH2:10]2)[O:16][CH2:22]1Participants
4
Procedure
The title compound is prepared from by the reaction of 1-cyclohexyloxy-2,2,6,6-tetramethylpiperidin-4-one and 1,1,1-tris(hydroxymethyl)ethane in the presence of p-toluenesulfonic acid.
Sources & evidence
- ORD record
- ord-56234b600bea40f0a7f78e10b66c5247
- Source dataset
- uspto-grants-1994_02
- Patent number
- US05286865
Reaction notes
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