HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 53638921, compound → HCID 86747587, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 53638921 | HCID 53638921 | — |
| Reactant | 3-[4-(1-Imidazolylmethyl)phenyl]-2-propen-1-yl 3-aminocrotonate | HCID 86747583 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | HCID 86747587 | HCID 86747587 | — |
Reaction Steps
297 mg (1 mM) of 3-{4-(1-imidazolylmethyl)phenyl}-2-propen-1-yl 3-aminocrotonate and 272 mg (1mM) of methyl 2-(3-trifluoromethylbenzylidene)acetoacetate were dissolved in 5 ml of toluene and refluxed for six hours. After cooling, the crystals produced were filtered off and recrystallized from methanol, whereby the captioned compound was obtained. The yield was 394 mg (71.5%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05286869 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-9c640a5fff5e49c2afc1a5b1e40e9863 |
| Source note | uspto-grants-1994_02 |