HuagongsheHuagongshe Chemistry Print Report · For research reference only
Iodoethane → HCID 22406593, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Iodoethane | HCID 6340 | — |
| Reactant | Allyl bromide | HCID 7841 | — |
| Reactant | (3-Methoxyphenyl)acetonitrile | HCID 88310 | — |
| Product | HCID 22406593 | HCID 22406593 | 46% |
Reaction Steps
The procedures described in the portion of Example 1 which is concerned with the preparation of starting materials were repeated except that 3-methoxyphenylacetonitrile was alkylated in turn with ethyl iodide and allyl bromide. The 2-allyl-2-(3-methoxyphenyl)butyronitrile so obtained was treated with boron tribromide to give the required starting material in an overall yield of 46% as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288742 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-5879d0a2b3aa49309709f06bc84ba5ef |
| Source note | uspto-grants-1994_02 |