反应详情

A suspension of N-acetyl-4-(pyrid-2-ylmethoxy)aniline (116 g; 480 mmol), prepared as in step 1, in 1000 mL 95% ethanol and 130 mL 10M aqueous KOH was refluxed for 2 days. The reaction was concentrated and diluted with water. The mixture was extracted with ethyl acetate. The extracts were dried over magnesium sulfate and concentrated to give 4-(pyrid-2-ylmethoxy)aniline as a brown oil.

1. concentrationThe reaction was concentrated
2. additiondiluted with water
3. extractionThe mixture was extracted with ethyl acetate
4. dry with materialThe extracts were dried over magnesium sulfate
5. concentrationconcentrated