2-Methoxy-4-Methylphenol → HCID 54266533, compound

HRID 1975825Notes

Reaction equation

HRID 1975825 reaction equation
[CH3:1][O:2][C:3]1[CH:8]=[C:7]([CH3:9])[CH:6]=[CH:5][C:4]=1[OH:10].C(N(CC)CC)C.[C:18](Cl)(=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1>>[C:18]([O:10][C:4]1[CH:5]=[CH:6][C:7]([CH3:9])=[CH:8][C:3]=1[O:2][CH3:1])(=[O:25])[C:19]1[CH:24]=[CH:23][CH:22]=[CH:21][CH:20]=1

Participants

4

Reactant 3

HCID 71442-Methoxy-4-MethylphenolHCID 7412Benzoyl chlorideHCID 8471Triethylamine

Product 1

HCID 54266533HCID 54266533, compound

Procedure

The synthesis of this compound proceeded in the same fashion as in Example 1 using 27.63 g (0.20 mol) of 2-methoxy-4-methyl phenol, 22.26 g (0.22 mol) of triethylamine and 28.11 g (0.20 mol) of benzoyl chloride. The product amounted to 46.78 g, m.p. 73°-75° C.

Workup

  1. customThe synthesis of this compound

Sources & evidence

ORD record
ord-44afea7a6f034eba93af764eb69df5b6
Source dataset
uspto-grants-1994_02
Patent number
US05288871

Reaction notes

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