HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 178524302, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 12506913 | HCID 12506913 | — |
| Reactant | HCID 178527813 | HCID 178527813 | — |
| Product | HCID 178524302 | HCID 178524302 | — |
Reaction Steps
The synthesis of this compound proceeded in the same fashion as in Example 3 using 6.79 g (0.045 mol) of 2-mercapto-1H-imidazo[4,5-c]pyridine, 1.14 g (0.0495 g atom) of sodium and 13.09 g (0.045 mol) of 2-(bromomethyl)phenyl benzoate. Purification of the crude material (12.75 g) by HPLC gave a product which on recrystallization from ethyl acetate had a m.p. 129°-132° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288871 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-8fd4caaedf3e4949a1cf76fb7658f23a |
| Source note | uspto-grants-1994_02 |