HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 178524401, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 10517659 | HCID 10517659 | — |
| Reactant | HCID 178527813 | HCID 178527813 | — |
| Product | HCID 178524401 | HCID 178524401 | 53.4% |
Reaction Steps
The synthesis of this compound proceeded in the same fashion as in Example 15 using 4.17 g (0.028 mol) of 2-mercapto-1H-imidazo[4,5-c]pyridine, 0.70 g (0.030 g atom) of sodium, and 8.04 g (0.028 mol) of 4-(bromomethyl)phenyl benzoate. The filtered precipitate (7.90 g) was recrystallized from methylene chloride to give 5.40 g of product, m.p. 171°-174° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288871 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-2206597e248c46bb8ff28b07e33edeb4 |
| Source note | uspto-grants-1994_02 |