HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium → HCID 54132819, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | HCID 19098804 | HCID 19098804 | — |
| Reactant | HCID 178527813 | HCID 178527813 | — |
| Product | HCID 54132819 | HCID 54132819 | — |
Reaction Steps
The synthesis of this compound proceeded in the same fashion as Example 15 using 1.66 g (0.011 mol) of 2-mercapto-1H-imidazo[4,5-c]pyridine, 0.28 g (0.012 g atom) of sodium and 4.51 g (0.011 mol) of 5-bromomethyl-benzene-1,3-diol dibenzoate. The crude material (4.2 g) when subjected to HPLC gave pure product (m.p. 209°-212° C.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288871 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-a7edbfb5ecdb4efab4abda29a54bb643 |
| Source note | uspto-grants-1994_02 |