HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thionyl Chloride → HCID 53883256, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thionyl Chloride | HCID 24386 | — |
| Reactant | (S)-2-methyl-3-phenylpropan-1-ol | HCID 11804940 | — |
| Product | HCID 53883256 | HCID 53883256 | — |
Reaction Steps
In accordance with the general procedure described in Example 8 (a), 22.5 g (0.15 mol) of (S)-2-methyl-3-phenylpropanol are reacted with 20.2 g (0.17 mol) of thionyl chloride, and the crude product is distilled under a high vacuum (18 torr) to give (b) (b.p. 110°-112° C.) as a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05288928 |
| Source dataset | uspto-grants-1994_02 |
| ORD ID | ord-43d5fd277fdc4062bb243f7770933b6e |
| Source note | uspto-grants-1994_02 |