Diethyl Ether → HCID 22237792, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of 2,3,3-trimethyl-3H-benzo[b]azole (2.39 g, 15 mmol) and 5-iodopentyl acetate (3.84 g, 15 mmol) in 1,2-dichlorobenzene (15 ml) were heated at 120° C. for 6 h and then cooled to ambient temperature. The mixture was then dripped into Et2O which precipitated the title compound as a red gum which was collected and used without any further purification in subsequent reactions.

Provenance & Evidence