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HRID1975921

反应详情

EQUATION

反应方程式

HRID 1975921 的结构方程式

REACTANTS

反应物

2
结构：S=C=NCC1CCCCC1
HCID142928

Cyclohexanemethyl isothiocyanate

C8H13NS

结构：Cl.Nc1cc(Cl)sc1S(N)(=O)=O
HCID68820626

未命名化合物

PRODUCTS

生成物

1
结构：Nc1cc(Cl)sc1S(=O)(=O)NC(=S)NCC1CCCCC1
HCID21999990

未命名化合物

收率 8%

PROCEDURE

实验过程

The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and cyclohexylmethyl isothiocyanate by a procedure analogous to the procedure described in example 3-a; a syrup was obtained (yield 8%), 1H-NMR (DMSO-d6): δ0.95 (m, 2H), 1.25 (m, 3H), 1.70 (m, 6H), 3.45 (d, 2H, CH2), 4.45 (br, HDO+NH), 6.65 (s, 1H, H4).

WORKUP

后处理

  1. customa syrup was obtained (yield 8%), 1H-NMR (DMSO-d6): δ0.95 (m, 2H), 1.25 (m, 3H), 1.70 (m, 6H), 3.45 (d, 2H, CH2), 4.45 (br, HDO+NH), 6.65 (s, 1H, H4)