HuagongsheHuagongshe Chemistry Print Report · For research reference only
(Isothiocyanatomethyl)Cyclohexane → N-(3-Amino-5-chloro-2-thienylsulfonyl)-N'-cyclohexylmethylthiourea
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | (Isothiocyanatomethyl)Cyclohexane | HCID 142928 | — |
| Reactant | 3-Amino-5-chlorothiophene-2-sulfonamide hydrochloride | HCID 68820626 | — |
| Product | N-(3-Amino-5-chloro-2-thienylsulfonyl)-N'-cyclohexylmethylthiourea | HCID 21999990 | 8% |
Reaction Steps
The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and cyclohexylmethyl isothiocyanate by a procedure analogous to the procedure described in example 3-a; a syrup was obtained (yield 8%), 1H-NMR (DMSO-d6): δ0.95 (m, 2H), 1.25 (m, 3H), 1.70 (m, 6H), 3.45 (d, 2H, CH2), 4.45 (br, HDO+NH), 6.65 (s, 1H, H4).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225310B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-82a4b86c0a7f45f3b88ab406aa8aa88c |
| Source note | uspto-grants-2001_05 |