(1-Isothiocyanatoethyl)benzene → HCID 11588885, compound

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Reaction Steps

The title compound was prepared from 3-amino-5-chlorothiophene-2-sulfonamide hydrochloride and D-α-methylbenzyl isothiocyanate by a procedure analogous to the procedure described in example 3-a (yield 96% impure product); 1H-NMR (DMSO-d6): δ1.46 (d, 3H, CH3), 5.36 (quint, 1H, CH), 6.45 (br s, 2H, NH2), 6.64 (s, 1H, H-4), 7.2-7.4 (m, 5H, ArH), 8.53 (br d, 1H, NH), 11.3 (br s, 1H).

Provenance & Evidence