HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 70246168, compound → HCID 20651504, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 70246168 | HCID 70246168 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20651504 | HCID 20651504 | 89.2% |
Reaction Steps
Ethyl 4-(3-nitro-6,11-dihydro-5H-cyclohepta[2,1-b:4,5- b′]dipyridin-11-yl)-1-piperidinecarboxylate ( 0.14gm, 0.367 mmol) was dissolved in 15 ml of ethanol. Palladium/carbon (10%, 20 mg) was added and the reaction mixture hydrogenated at 50 psi of hydrogen for 2 hours. The palladium was filtered and the ethanol evaporated to give 0.12 gm of the title product. FABMS (M+1)=367
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06225322B1 |
| Source dataset | uspto-grants-2001_05 |
| ORD ID | ord-f4d38900be3b4399afc61b79f63470ca |
| Source note | uspto-grants-2001_05 |